Rotational Viscometer (Brookfield Viscometer)

Principle of Rotational Viscometer (Brookfield Viscometer):

Rotational Viscometer (Brookfield Viscometer) (2)

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  • Measures the torque required to rotate a spindle at constant speed in the sample.
  • The resistance to rotation is a function of the sample’s viscosity.
  • $\eta \propto \frac{\text{Torque}}{\text{Angular velocity}}$

Types:

  1. Couette-type (coaxial cylinder):

    • Inner cylinder rotates, outer is stationary or vice versa.
    • Used for both Newtonian and non-Newtonian fluids.
  2. Cone and Plate viscometer:

    • Ideal for small sample volumes.
    • High accuracy in measuring shear stress and shear rate.
  3. Brookfield viscometer:

    • Common in pharmaceutical QC labs.
    • Measures torque on rotating spindle at different speeds.
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Applications:

  • Suitable for non-Newtonian systems.
  • Can measure:
    • Thixotropy (using up-and-down shear curve)
    • Pseudoplastic and plastic behavior
    • Viscosity at various shear rates

Advantages:

  • Very versatile
  • Measures both Newtonian and non-Newtonian behavior
  • Can study time-dependent properties (like thixotropy)
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Limitations:

  • Calibration and spindle choice are critical
  • Requires trained handling

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